Low temperature solution growth (LTSG) in one of the most efficient andsimplest processes. This can be employed for crystal growth from solutions. The casein handling and the readiness in its miscibility with the solvents it attractive techniquefor crystal growth. Crystal growth evaporation method is a simplest method used forthe preparation of crystal to study their structure. The crystals have been analysis FT -IR and Vickers micro hardness test analysis. Sodium chloride doped Glysine weregrow by slow evaporation method.